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- W2073287546 abstract "Abstract The ligand N′-[(2-methoxyphenyl)carbonothioyl]pyridine-2-carbohydrazide (H2mcph), having NNS donor sequence, has been found to form [Ni(Hmcph)2]·CH2Cl2·0.5C6H6 and [Mn(Hmcph)2]·2H2O which have been characterized by spectroscopic and spectrometric techniques including magnetic susceptibility measurements and single crystal X-ray of both complexes. The compounds crystallize in the triclinic and monoclinic systems with the space group P 1 ¯ and P2(1)/c, respectively with a distorted octahedral geometry about the M(II) center. The ligand is coordinated through the ring nitrogen, hydrazinic N and thione sulfur. The hydrazinic nitrogen coordinates with a shorter M–N distance than the ring nitrogen and the bond lengths in the chelate ring systems are intermediate between single and double bond distances, suggesting considerable delocalization of charge." @default.
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- W2073287546 date "2010-05-01" @default.
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- W2073287546 title "Ni(II) and Mn(II) complexes of NNS tridentate ligand N′-[(2-methoxyphenyl)carbonothioyl]pyridine-2-carbohydrazide (H2mcph): Synthesis, spectral and structural characterization" @default.
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- W2073287546 doi "https://doi.org/10.1016/j.poly.2010.03.005" @default.
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