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- W2073320910 abstract "A dihydroxyterphenylphosphine bearing cyclohexyl groups on the phosphorus atom (Cy-DHTP) was found to be a powerful ligand for the palladium-catalyzed one-pot synthesis of substituted benzo[b]furans from 2-chlorophenols and terminal alkynes. This catalyst system was also applicable to the sequential one-pot synthesis of disubstituted benzo[b]furans from dichlorophenols via the Suzuki–Miyaura cross-coupling of chlorobenzo[b]furan with boronic acids. The use of two ligands, Cy-DHTP and XPhos, is the key to promoting the reactions. Mechanistic studies suggest that the Pd–Cy-DHTP catalyst is the active species in the Sonogashira cross-coupling step, while the Pd–XPhos catalyst accelerates the Suzuki–Miyaura cross-coupling step." @default.
- W2073320910 created "2016-06-24" @default.
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- W2073320910 date "2013-08-30" @default.
- W2073320910 modified "2023-09-26" @default.
- W2073320910 title "One-Pot Synthesis of Substituted Benzo[<i>b</i>]furans from Mono- and Dichlorophenols Using Palladium Catalysts Bearing Dihydroxyterphenylphosphine" @default.
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- W2073320910 doi "https://doi.org/10.1021/jo401503t" @default.
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