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• W2073574976 abstract "Wide-angle X-ray data point to a three-phase structure in isotropic and drawn specimens of a homogeneous poly(ethylene-co-octene) (7.3 mol % 1-octene). In addition to the amorphous halo, the unoriented polymer exhibits Bragg reflections characteristic of the orthorhombic crystalline phase and an additional reflection that is assigned to the hexagonal mesophase. On stretching 800%, the degree of crystallinity increases from ∼25% to ∼50%, due mainly to the formation of smaller hexagonal crystallites, while the proportions of the orthorhombic and amorphous phases decline. Small-angle X-ray data reveal a distinct long period, pointing to the existence of lamellae that become oriented perpendicular to the draw direction. On releasing the specimen, there is a considerable permanent set (∼350% extension), and the crystallinity declines to ∼30% as the hexagonal crystallites appear to revert to the amorphous structure. The results suggest that the hexagonal mesophase is formed by chain segments that have octene side chains, once these segments become oriented by deformation." @default.
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• W2073574976 date "1999-05-06" @default.
• W2073574976 modified "2023-10-17" @default.
• W2073574976 title "Wide- and Small-Angle X-ray Analysis of Poly(ethylene-<i>c</i><i>o</i>-octene)" @default.
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• W2073574976 doi "https://doi.org/10.1021/ma9818331" @default.
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