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• W2073661637 abstract "We here report on the influence of heteronuclear dipolar decoupling on the (27)Al 3QMAS, 5QMAS, and the double-quantum filter-satellite-transition magic-angle spinning (DQF-STMAS) spectra of a strongly dipolar-coupled system, gibbsite. The requirements for heteronuclear dipolar decoupling increase with the order of coherence evolving in the indirect dimension of a two-dimensional (2D) experiment. The isotropic line width of the high-resolution 2D spectra, in samples like gibbsite, is composed of four parts: the distribution of isotropic shifts (delta(ISO), delta(QIS)), the homogeneous broadening related to the proton-proton flip-flop terms, the (27)Al-(27)Al homonulcear dipolar couplings, and the (1)H-(27)Al heteronuclear dipolar couplings. It is shown that, even in the case of gibbsite, where a strong proton-proton bath exists, the main resolution limiting factor in these experiments resides in the (1)H-(27)Al dipolar interaction." @default.
• W2073661637 created "2016-06-24" @default.
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• W2073661637 date "2008-08-21" @default.
• W2073661637 modified "2023-10-09" @default.
• W2073661637 title "Heteronuclear dipolar decoupling effects on multiple‐quantum and satellite‐transition magic‐angle spinning NMR spectra" @default.
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• W2073661637 doi "https://doi.org/10.1002/mrc.2286" @default.
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