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• W2073687334 abstract "Abstract The reaction of [Pt(μ-Cl)(κ,η 2 -COE-MeO)] 2 ( 2 ) (COE-MeO = 2-methoxy-5-cycloocten-1-yl) with trispyrrolylphosphine yields [PtCl{P(pyrl) 3 }(κ,η 2 -COE-MeO)] ( 3 ), in contrast to the crown-cycle complex [Pd(μ-Cl) {P(pyrl) 3 }] 8 ( 1 ) obtained with the analogous palladium complex. The different reactivity has been explained in terms of the higher lability of the carbon–carbon double bond in the starting palladium compound, as compared with the related platinum derivative. The reaction of 1 with the ligand 2-[(pyridin-2-ylmethylene)aminophenol], (HNN′O), in the presence of thalium salt and NEt 3 , yields the complex [Pd(κ 3 N , N ′, O -py-CH N-C 6 H 4 O)(P(O)(pyrl) 2 )] ( 5 ), which contains, for the first time, a di( N -pyrrolyl)phosphonato- P ligand. Treatment of [PdCl(κ 3 N , N ′, O -py-CH N-C 6 H 4 O)] with P(pyrl) 3 gives the amido derivative [PdCl{κ 3 P , N , N -(P(pyrl) 2 -O-C 6 H 4 -N-CH(CH 2 -CO-CH 3 )-py)}] ( 7 ), which displays a N–Pd–P–O–C 2 six-membered metallacycle. In addition, the latter compound has been able to insert an acetone molecule into its framework. The crystal structures of 5 and 7 were solved by X-ray diffraction analysis." @default.
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• W2073687334 date "2007-08-01" @default.
• W2073687334 modified "2023-10-18" @default.
• W2073687334 title "About the different reactivity of dinuclear palladium and platinum compounds with trispyrrolylphosphine: Synthesis and X-ray crystallographic results of new palladium complexes containing P–pyrrolyl bonds" @default.
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• W2073687334 doi "https://doi.org/10.1016/j.jorganchem.2007.05.038" @default.
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