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- W2073707942 abstract "When immersed in solutions containing Cu(II) cations, the microporous metal–organic material P11 ([Cd4(BPT)4]·[Cd(C44H36N8)(S)]·[S], BPT = biphenyl-3,4′,5-tricarboxylate) undergoes a transformation of its [Cd2(COO)6]2– molecular building blocks (MBBs) into novel tetranuclear [Cu4X2(COO)6(S)2] MBBs to form P11-Cu. The transformation occurs in single-crystal to single-crystal fashion, and its stepwise mechanism was studied by varying the Cd2+/Cu2+ ratio of the solution in which crystals of P11 were immersed. P11-16/1 (Cd in framework retained, Cd in encapsulated porphyrins exchanged) and other intermediate phases were thereby isolated and structurally characterized. P11-16/1 and P11-Cu retain the microporosity of P11, and the relatively larger MBBs in P11-Cu permit a 20% unit cell expansion and afford a higher surface area and a larger pore size." @default.
- W2073707942 created "2016-06-24" @default.
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- W2073707942 date "2013-04-10" @default.
- W2073707942 modified "2023-10-16" @default.
- W2073707942 title "Stepwise Transformation of the Molecular Building Blocks in a Porphyrin-Encapsulating Metal–Organic Material" @default.
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- W2073707942 doi "https://doi.org/10.1021/ja4015666" @default.
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