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- W2073762009 abstract "A method of increased sensitivity for hydrogen enthalpimetry of olefins in mumole quantities is reported. The method depends on a linear relationship between the amount of alkene present and the heat given off on hydrogenation at slightly more than 2 atm pressure over palladium catalyst on charcoal. Least-squares analysis of the results shows that the measured heat effect is a linear function of amount of alkene taken, with a relative standard deviation of 1-3% for samples ranging in size from 1.4 to 37.5 mumole. Extension of the method to samples in submicromolar quantities was only partially successful; in a series of measurements extending to a minimum amount of 0.64 mumole, the relative standard deviation rose to 9.6%." @default.
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- W2073762009 title "Enthalpimetry of non-aromatic alkenes" @default.
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- W2073762009 doi "https://doi.org/10.1016/0039-9140(73)80274-7" @default.
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