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- W2073875971 abstract "The title compounds, tris(1,10-phenanthroline-κ 2 N , N ′)iron(II) bis(2,4,5-tricarboxybenzoate) monohydrate, [Fe(C 12 H 8 N 2 ) 3 ](C 10 H 5 O 8 ) 2 ·H 2 O, (I), and tris(2,2′-bipyridine-κ 2 N , N ′)iron(II) 2,5-dicarboxybenzene-1,4-dicarboxylate–benzene-1,2,4,5-tetracarboxylic acid–water (1/1/2), [Fe(C 10 H 8 N 2 ) 3 ](C 10 H 4 O 8 )·C 10 H 6 O 8 ·2H 2 O, (II), were obtained during an attempt to synthesize a mixed-ligand complex of Fe II with an N-containing ligand and benzene-1,2,4,5-tetracarboxylic acid via a solvothermal reaction. In both mononuclear complexes, each Fe II metal ion is six-coordinated in a distorted octahedral manner by six N atoms from three chelating 1,10-phenanthroline or 2,2′-bipyridine ligands. In compound (I), the Fe II atom lies on a twofold axis in the space group C 2/ c , whereas (II) crystallizes in the space group P 2 1 / n . In both compounds, the uncoordinated carboxylate anions and water molecules are linked by typical O—H...O hydrogen bonds, generating extensive three-dimensional hydrogen-bond networks which surround the cations." @default.
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- W2073875971 date "2012-08-18" @default.
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- W2073875971 title "Tris(1,10-phenanthroline-κ2N,N′)iron(II) bis(2,4,5-tricarboxybenzoate) monohydrate and tris(2,2′-bipyridine-κ2N,N′)iron(II) 2,5-dicarboxybenzene-1,4-dicarboxylate–benzene-1,2,4,5-tetracarboxylic acid–water (1/1/2)" @default.
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- W2073875971 doi "https://doi.org/10.1107/s0108270112034567" @default.
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