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- W2074004799 abstract "The temperature-dependent 13C NMR spectra of a series of para-substituted 1-phenyl-3,3-tetramethylenetriazenes have been analyzed by the band width method. Electron-donating substituents clearly accelerate the rate of rotation about the N-2N-3 bond in the triazenes; electron withdrawers retard that motion. The exchange averaging process observed in the carbon spectra obeys a linear free energy relationship when Hammett σ* parameters are used in the correlation. These results corroborate those already obtained by analysis of 1H NMR spectra of similar triazenes, regarding the likely contribution of a 1,3-dipolar resonance form to the ground state of the molecule." @default.
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- W2074004799 title "Dynamic13C NMR: A study of aryl-substituted 1-phenyl-3,3-tetramethylenetriazenes" @default.
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- W2074004799 doi "https://doi.org/10.1002/mrc.1260230206" @default.
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