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- W2074005089 abstract "Abstract The determination of selenium(IV) by voltammetry through the formation of a piazselenol with 3,3′-diaminobenzidine (DAB) is described. At pH 1.5 and with a large excess of DAB, the formation of piazselenol is quantitative. In a borate-buffered electrolyte at pH 9, the piazselenol gives reduction peaks at potentials of −0.64 V and −0.82 V vs. SCE. The influence of DAB concentration on the sensitivity of the method is discussed. The calibration graphs are linear over the range 0–200 μg l−1 Se(IV) and the detection limit is 0.10 μg l−1. Copper(II) and lead(II) are tolerated in 500-fold amounts; the method is applicable to the determination of selenium in NBS Oyster Tissue." @default.
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- W2074005089 date "1987-01-01" @default.
- W2074005089 modified "2023-09-26" @default.
- W2074005089 title "Determination of selenium(IV) by differential pulse voltammetry of the 3,3′-diaminobenzidine piazselenol" @default.
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- W2074005089 doi "https://doi.org/10.1016/s0003-2670(00)85320-9" @default.
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