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- W2074057791 abstract "A low temperature (60 or 95 °C), “one-pot” procedure for aqueous precipitation of layered manganese oxide core@shell particles is developed, based on the reaction between MnO4− and Mn2+. Characterization of the particles was carried out using powder XRD, nitrogen adsorption−desorption, FESEM, TEM, and electron diffraction. Textural and morphological tailoring is achieved through various experimental parameters, with the specific surface area adjusted between 15 and 110 m2 g−1 while a ball-like or sheetlike shape is selectively obtained. The synthesis is based on a two-step precipitation process, with the first stage involving in situ seeding and enabling shape control via adjustment of the initial acidity. Hierarchical core−corona particles are obtained through a second slower heterogeneous nucleation stage, controlled by reactant ratio, aging time, temperature, and acidity of the aging medium." @default.
- W2074057791 created "2016-06-24" @default.
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- W2074057791 date "2008-01-01" @default.
- W2074057791 modified "2023-10-14" @default.
- W2074057791 title "Design of Hierarchical core-corona architectures of layered manganese oxides by aqueous precipitation" @default.
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