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- W2074090030 abstract "The kinetics of reaction of coupons of annealed and unannealed titanium with pure sulphur vapour have been investigated by a thermogravimetric method over the temperature range 450–550 °C. The sulphurization kinetics for the annealed metal were parabolic and for the unannealed titanium they were pseudo-parabolic. The apparent activation energy calculated from the parabolic rate constants was 27 kcal mol−1. For the annealed metal parabolic kinetics were observed for total sulphur pressures in the range 0.2–300 Torr; the parabolic rate constant increased as the square root of the partial pressure of S2. The only reaction product detected under all experimental conditions was Ti1 + xS2, which microprobe analysis showed to be slightly metal-rich. For a given temperature and sulphur pressure the sulphurization rate was independent of the presence of inert gas or hydrogen but was strongly and erratically influenced by the presence of oxygen. The sulphurization process is discussed in terms of a reaction controlled by the diffusion of titanium through the thickening Ti1 + xS2 scale." @default.
- W2074090030 created "2016-06-24" @default.
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- W2074090030 date "1977-02-01" @default.
- W2074090030 modified "2023-09-26" @default.
- W2074090030 title "The reaction of titanium with sulphur vapour" @default.
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- W2074090030 doi "https://doi.org/10.1016/0022-5088(77)90090-x" @default.
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