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- W2074202408 abstract "The synthesis of enantiomeric phytoprostane B1 type II methyl esters has been accomplished in approximately 30% overall yield via two basic transformations starting from 3-[(dimethoxyphosphoryl)methyl]cyclopentenone as a key reagent. They include ethylation of the ring C(2) carbon and a Horner olefination reaction using the phosphonate moiety at C(3). The novel components of the Horner reaction, the enantiomeric methyl 9-formyl-9-hydroxynanoates, were easily prepared from racemic methyl 9-hydroxy-10-undecenoate via asymmetric Sharpless epoxidation (kinetic resolution) followed by ozonolysis." @default.
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- W2074202408 date "2011-10-01" @default.
- W2074202408 modified "2023-09-26" @default.
- W2074202408 title "A concise approach to both enantiomers of phytoprostane B1 type II" @default.
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- W2074202408 doi "https://doi.org/10.1016/j.tetasy.2011.10.005" @default.
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