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- W2074388204 abstract "The title copolymers have been prepared by the free-radical-initiated copolymerization of 2-chlorostyrene (2-ClSt), 4-chlorostyrene (4-ClSt) and 2,6-dichlorostyrene (2,6-DClSt) with maleic anhydride (MAn) in toluene at 65°C. Copolymers of chlorinated styrenes with MAn prepared under different monomer-to-monomer ratios in the feed have alternating composition. In all cases, the mixture of comonomers forms charge-transfer complex monomers (CTC). The initial rate of copolymerization increases with the increase of electron donors in the comonomer feed, and the highest rates were at the equimolar ratios of comonomers in the feed. The thermal stability of the polymers was measured by thermogravimetric analysis in nitrogen. Homopolymers decompose by a one-step mechanism, while copolymers are more thermostable and decompose by a two-step mechanism. Glass transition temperatures (Tgs) of homopolymers are lower than Tgs of copolymers. The number and weight average molecular weights of chlorinated copolymers are hig..." @default.
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- W2074388204 date "2001-01-01" @default.
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- W2074388204 title "FREE-RADICAL-INITIATED COPOLYMERIZATION OF 2-CHLOROSTYRENE, 4-CHLOROSTYRENE, AND 2,6-DICHLOROSTYRENE WITH MALEIC ANHYDRIDE" @default.
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- W2074388204 doi "https://doi.org/10.1081/ma-100103347" @default.
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