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- W2074496212 abstract "The anodic chlorination of anisole on an α-cyclodextrin (α-CD) chemically modified electrode via ether linkage (α-CD-CME) and a naked graphite electrode with α-CD or β-CD in solution was studied. In the presence of CD, the p- to o-chloroanisole ratio, formed in the reaction, was higher than that in the absence of CD since o-positions of anisole included in CD are blocked by the inner wall of CD. Especially, α-CD had a profound effect on the p-isomer formation. Increasing the concentration of NaCl added as a supporting electrolyte in the presence of α-CD resulted in a decrease in the ratio because of the inhibition effect of chloride ion on the inclusion of anisole in α-CD, whereas such effect was small in the presence of β-CD. The ratio on α-CD-CME was slightly higher than that on the naked electrode. This indicates that α-CD was introduced on the graphite surface but the surface coverage of α-CD was low, which was in accord with the ESCA results of α-CD-CME." @default.
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- W2074496212 date "1979-12-01" @default.
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- W2074496212 title "Selective Electrosyntheses on Chemically Modified Electrode. II. Anodic Chlorination of Anisole with Cyclodextrin on Electrode Surfaces and in Solution" @default.
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- W2074496212 doi "https://doi.org/10.1246/bcsj.52.3692" @default.
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