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- W2074527982 abstract "Calcium deficient hydroxyapatites were impregnated to varying degrees with fluoride in very dilute solutions of NaF at room temperature. Ca/P ratios were determined before and after fluoridation. Phosphate loss upon fluoridation was consistent with an initial mechanism of OH − vacancy filling by F − , with equivalent amounts of PO 4 3− ions escaping to restore charge balance. Infrared measurements confirmed previous evidence of OH/F exchange and the formation of [Formula: see text] hydrogen bonds, which increased with progressive thermal activation, considerable exchange having occurred already at 120 °C and possibly below. The first signs of lattice collapse occurred near 600 °C, with the fluorided sample exhibiting somewhat better stability." @default.
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- W2074527982 date "1974-12-15" @default.
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- W2074527982 title "The Fluoridation of Nonstoichiometric Calcium Hydroxyapatite. An Infrared Study" @default.
- W2074527982 doi "https://doi.org/10.1139/v74-597" @default.
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