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Matches in SemOpenAlex for { <https://semopenalex.org/work/W2074668854> ?p ?o ?g. }

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• W2074668854 abstract "A sensitive and specific liquid chromatographic-tandem mass spectrometric (LC-MS-MS) method has been validated for the measurement of YF476 in human plasma. The method involves a simple liquid-liquid extraction procedure, chromatography of the extracts on a C(18) column, atmospheric pressure chemical ionisation and detection in the multiple reaction monitoring mode. The calibration line was linear over the concentration range 0.1 ng/ml (the limit of quantification) to 25.0 ng/ml. Intra- and inter-batch precision was <14% and intra- and inter-batch accuracy was <11% over the entire calibration range. The bioanalytical method is robust and has been used for the analysis of many samples from human subjects involved in early clinical studies (Phase I)." @default.
• W2074668854 created "2016-06-24" @default.
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• W2074668854 date "2002-06-01" @default.
• W2074668854 modified "2023-10-10" @default.
• W2074668854 title "Validation of a liquid chromatographic–tandem mass spectrometric method for the measurement of (R)-1-[2,3-dihydro-2-oxo-1-pivaloylmethyl-5-(2-pyridyl)-1H-1,4-benzodiazepin-3-yl]-3-(3-methylaminophenyl)urea (YF476) in human plasma" @default.
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• W2074668854 doi "https://doi.org/10.1016/s1570-0232(02)00118-6" @default.
• W2074668854 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/12007777" @default.
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