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- W2074691569 abstract "In two previous papers we described: (a) the reduction of O2 and CO2, in the presence of each other, in an aprotic solvent with minimal cross-interference between the competing O2 and CO2 reduction reactions; (b) a practical Clark-type membrane-covered sensor for the simultaneous measurement of O2 and CO2. The sensor comprised a gold disc microelectrode, housed in a PTFE holder and covered with a PTFE membrane, with dimethyl sulphoxide as the solvent and with an Ag quasi-reference electrode. In this new work, we describe the reduction of O2 and N2O, in the presence of each other, with this same sensor when the microelectrode was first unshielded and then membrane-covered. No cross-interference from the two reactions was evident, and the problem N2O bubble build-up on the microelectrode surface, from the reduction of N2O, was minimised by sweeping the polarising voltage from 0 to −2.4 V (Ag) at a typical sweep rate of 0.1 to 0.5 V s−1. The O2 and N2O concentrations were determined from the limiting currents of the well-separated O2 and reduction N2O waves. We also demonstrated that the addition of up to 100% v/v H2O to the solvent did not appear to comprimise the ability of the sensor to analyse O2 and N2O simultaneously." @default.
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- W2074691569 date "1997-04-01" @default.
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- W2074691569 title "The development of new microelectrode gas sensors: an odyssey. Part III. O2 and N2O reduction at unshielded and membrane-covered gold microdisc electrodes" @default.
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- W2074691569 doi "https://doi.org/10.1016/s0022-0728(96)04993-5" @default.
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