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- W2074773182 abstract "Abstract An efficient total synthesis of ( S )‐14‐azacamptothecin has been accomplished in 10 steps and 56 % overall yield from 5 H ‐pyrano[4,3‐d]pyrimidine 8 . A mild Hendrickson reagent‐triggered intramolecular cascade cyclization, a highly enantioselective dihydroxylation, and an efficient palladium‐catalyzed transformation of an O ‐allyl into N ‐allyl group are the key steps in the synthesis. This work provides a much higher overall yield than the previous achievement and shows sound flexibility for the further applications that will lead to new bioactive analogues." @default.
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- W2074773182 date "2010-05-28" @default.
- W2074773182 modified "2023-10-18" @default.
- W2074773182 title "Efficient Total Synthesis of (S)-14-Azacamptothecin" @default.
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- W2074773182 doi "https://doi.org/10.1002/asia.201000073" @default.
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