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- W2074777287 abstract "The selenium-containing cluster [Ru4(µ4-Se)2(CO)8(µ-CO)3]1 may be readily prepared by vacuum pyrolysis of [Ru3(CO)12] with PhSeSePh at 185 °C. The subsequent reaction of 1 with the bidentate phosphine ligand bis(diphenylphosphino)acetylene (dppa) affords the orange triruthenium cluster [Ru3(µ3-Se)2(CO)7(dppa)]2, in 80% yield. Complex 2 crystallises in the space group P with a= 12.059(3), b= 12.274(3), c= 13.172(5)A, α= 66.78(2), β= 83.21(3), γ= 89.30(2)° and Z= 2. Treatment of complex 1 with triphenylantimony, SbPh3, yields the antimony-substituted cluster [Ru4(µ4-Se)2(CO)10(SbPh3)]3, in quantitative yield. Complex 3 crystallises in the space group P with a= 9.474(4), b= 12.456(3), c= 14.913(5)A, α= 91.89(2), β= 93.88(3), γ= 109.99(3)° and Z= 2. Reaction of cluster 1 with carbon monoxide at room temperature and 70 atm affords the triruthenium selenido-bridged cluster [Ru3(µ3-Se)2(CO)9]4. Complex 4 crystallises in the space group P with a= 6.887(3), b= 9.606(7), c= 13.567(9)A, α= 82.48(6), β= 84.91(4), γ= 68.85(5)° and Z= 2." @default.
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- W2074777287 title "The chemistry of the selenium-containing cluster [Ru4(µ4-Se)2(CO)8(µ-CO)3]: crystal structures of [Ru3(µ3-Se)2(CO)7(Ph2PC2PPh2)], [Ru4(µ4-Se)2(CO)10(SbPh3)] and [Ru3(µ3-Se)2(CO)9]" @default.
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- W2074777287 doi "https://doi.org/10.1039/dt9920003411" @default.
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