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- W2074850161 abstract "In initiator/TiCl4-initiated cationic polymerization, studies of the dynamics of reaction systems must be conducted within a certain range of the concentration ratio between the initiator and TiCl4. The current study explored the range of the concentration ratio of CH2Cl2/TiCl4 in the cationic polymerization of pyrolysis gasoline. AlCl3 and TiCl4 were used as the catalysts. The compositions and iodine values of the light components were analyzed using gas chromatography-mass spectrometry and the iodine–alcohol method, respectively. The molecular weights of the resulting polymers were analyzed using gel permeation chromatography, and their compositions were analyzed using Fourier transform infrared spectroscopy and nuclear magnetic resonance spectroscopy. In the CH2Cl2/TiCl4-initiated cationic polymerization of multiple-olefin-containing C9 pyrolysis distillate, the CH2Cl2/TiCl4 ratio needed to be ≤1 for effective initiation. A low concentration of olefins in the reaction systems yielded satisfactory polymerization. The temperature for the CH2Cl2/TiCl4-initiated polymerization of the C9 pyrolysis distillate was 50 °C, and the amount of TiCl4 was 1.5%. The olefins in the C9 pyrolysis distillate were effectively isolated from the saturated solutions through cationic polymerization, and the resulting light oil was transparent and colorless. The analysis of the resulting polymers suggested the secondary polymerization of low-molecular-weight polymers after the addition of initiator/TiCl4." @default.
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- W2074850161 date "2014-01-01" @default.
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- W2074850161 title "Initiator/TiCl4 initiated cationic polymerization of pyrolysis gasoline distillate" @default.
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- W2074850161 doi "https://doi.org/10.1039/c4ra02945c" @default.
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