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- W2074991871 abstract "Abstract A hydrated single crystal of zeolite X with unit-cell composition Na 92 Si 100 Al 92 O 384 , exclusive of water molecules, 0.14 mm in cross-section, was ion exchanged at 23°C with flowing 0.1 M aqueous TlNO 3 for 90 s. Its structure, determined crystallographically, showed that 74(4) of the 92 Na + ions per unit cell had been replaced by Tl + . A second crystal was treated similarly for 900 s; this time 83(1) Tl + ions were found. Kim et al. had found 91(1) Tl + ions after 7.0 days =6.0 × 10 5 s [Y. Kim, Y.W. Han, K. Seff, Zeolites 18 (1997) 325]. These results can be fit relatively well to a simple fourth-order rate law with k = 6.25 × 10 −7 (No. of Na + per unit cell) −3 s −1 . For crystals of such size, which are important for X-ray crystallography, days may not be enough time to reach an ion-exchange end point by these methods for some ions." @default.
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- W2074991871 date "2000-09-01" @default.
- W2074991871 modified "2023-09-24" @default.
- W2074991871 title "Rate of Tl+ exchange into single crystals of zeolite X" @default.
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- W2074991871 doi "https://doi.org/10.1016/s1387-1811(00)00195-5" @default.
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