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- W2075303915 abstract "A method for the determination in vivo of the benzylpenicillin residues in ovine milk at low levels was described. Two groups of Sardinian breed sheep were treated with a dose of penicillin G sodium salt by intramammary infusion and intramuscular administration respectively. The residues were detected by isocratic HPLC method of the extracts obtained from a previous cleanup procedure. Linear calibration plots were obtained over a large concentration range of 1 mg ml−1–10 ng ml−1, with correlation coefficients greater than 0.998. Recoveries between 78.6 and 87.3% were obtained. Limit of detection (LOD) and limit of determination (LOQ) were 2.6 and 8.8 ng ml−1 respectively. This method would be useful for routine monitoring of penicillin G residues in ovine dairy milk." @default.
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- W2075303915 date "1998-08-01" @default.
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- W2075303915 title "Monitoring of benzylpenicillin in ovine milk by HPLC" @default.
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- W2075303915 doi "https://doi.org/10.1016/s0731-7085(97)00245-8" @default.
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