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- W2075322618 abstract "AbstractThe recovery of TiCl4 from the slurry formed in raw titanium tetrachloride was studied and a new environment friendly process was developed by selective extraction, gravity sedimentation and distillation. The results from the experiment confirmed that this technology was an effective method for the recovery of TiCl4 from the slurry. During selective extraction and gravity sedimentation process, dichloromethane was considered to be the best extractant comparing to chloroform and carbon tetrachloride. Meanwhile, nearly 91% of TiCl4 was recovered by extracting with dichloromethane in the solvent/slurry (L/S) ratio of 2 : 1 for 5 min. The study of gravity sedimentation also indicates that the concentration of TiCl4 in the extracting solution should be controlled to ensure the separation of extracting solution and residue by gravity sedimentation. Raman spectroscopy analysis and relative volatilities of CH2Cl2 and TiCl4 indicates that titanium tetrachloride and dichloromethane can be separated effectiv..." @default.
- W2075322618 created "2016-06-24" @default.
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- W2075322618 date "2014-03-13" @default.
- W2075322618 modified "2023-09-27" @default.
- W2075322618 title "Recovery of TiCl4from the slurry formed in raw titanium tetrachloride by extraction with halogenated hydrocarbon" @default.
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- W2075322618 doi "https://doi.org/10.1179/1879139514y.0000000123" @default.
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