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- W2075324518 startingPage "2274" @default.
- W2075324518 abstract "The crystals of butein monohydrate isolated from Dahlia variabilis are monoclinic. The unit cell, with dimensions of a=10.89, b=28.88, c=4.29 Å, and β=96.7°, contains four molecules, and the space group is P21/n. An approximate structure was obtained by applying the symbolic addition procedure. The structural parameters were refined by the block-diagonal least-squares method, and the final R factor for 1063 observed reflexions was 0.171. In the molecule, the C(7)–C(8) double bond and the C(9)–O(3) carbonyl group take the s-cis conformation with respect to the C(8)–C(9) single bond. The A phenyl group and the exocyclic atoms (C(7)∼O(3)) are nearly coplanar, and this plane makes a dihedral angle of 15.6° with that of the B phenyl group. The molecules build up a three-dimensional net through the hydrogen bonds. There is also an intramolecular hydrogen bond between O(3) and O(4)." @default.
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- W2075324518 date "1972-08-01" @default.
- W2075324518 modified "2023-09-26" @default.
- W2075324518 title "The Crystal and Molecular Structure of Butein Monohydrate, Isolated from<i>Dahlia variabilis</i>" @default.
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- W2075324518 doi "https://doi.org/10.1246/bcsj.45.2274" @default.
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