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- W2075384245 abstract "Four new bimetallic model precursors of copper-zinc oxide catalysts for methanolization were prepared: Zn(NH3)2Cu(CN)3 (ZCA), [Zn(en)3]6[Cu5(CN)17]·nH2O (n = 8.4) (ZCE3), Zn(en)Cu(CN)3 (ZCE1) and [Zn1 − xCux(en)][Cu(CN)3] (ZCCE1). The new compounds were characterized by elemental analysis, IR spectroscopy, and thermal analysis under dynamic conditions. Thermal stability increases in the order ZCE3 (65) < ZCA (120) < ZCE1 or ZCCE1 (155°C). Thermal decomposition in air proceeds via the following steps: dehydration (if water molecules are present), deamination, redox decomposition of the cyano groups with formation of metallic copper and ZnO, and finally re-oxidation of copper to CuO. In the case of en-containing compounds an unexplained phase transition was observed at 800°C." @default.
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- W2075384245 date "1996-04-01" @default.
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- W2075384245 title "Copper-zinc oxide catalyst. Part II. Preparation, IR characterization and thermal properties of novel bimetallic precursors" @default.
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- W2075384245 doi "https://doi.org/10.1016/0040-6031(95)02736-x" @default.
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