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- W2075520797 abstract "Abstract PFG NMR diffusion measurements were carried out to determine the effect of solvent on intracrystalline reactant diffusivities and on 1-hexene epoxidation rates in TS-1 catalyst. Using n -hexane in silicalite as a mimic for the TS-1 system, the self-diffusivity of n -hexane in silicalite was found to be 24% higher in methanol solvent than in acetonitrile solvent and 45% higher than in acetone solvent. The presence of trace Al did not affect n -hexane diffusivity. Based on analysis of the Weisz modulus for a slab morphology, the 1-hexene epoxidation reaction in TS-1 was found to be diffusion limited only if the crystal size is at least 38 μm in the methanol system." @default.
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- W2075520797 date "2006-12-01" @default.
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- W2075520797 title "Is 1-hexene epoxidation in TS-1 diffusion limited in different solvents?" @default.
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- W2075520797 doi "https://doi.org/10.1016/j.catcom.2006.04.008" @default.
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