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- W2076103246 abstract "Reaction of M′Cl2(bpy)2 (M′ = Co, Ni, Mn) with (PPh4)2MS4 (M = Mo, W) affords MS4M′(bpy)2. Crystals of WS4Co(bpy)2,12dmf are monoclinic space group P21/n (a = 12.458, b = 21.862, c = 10.164 Å and β = 100.0°, Z = 4, R = 0.039 for 5414 independent data). The coordination geometry around the cobalt atom is octahedrally distorted with two bipyridyl groups and two sulfur atoms being cis to each other. Reaction of M′Cl2(bpy)2 with [NEt4]2[(MS4)2M″] (M″ = Pd, Pt) gives [M′(bpy)3][(MS4)2M″]. Crystals of [Ni(bpy)3][(WS4)2Pd] are triclinic, space group P1 (a = 12.771, b = 14.838, c = 12.077 Å, α = 72.9, β = 116.9 and γ = 96.1°, Z = 2, R = 0.042 for 3842 independent data). In the anionic species, the central palladium atom is coordinated by two chelating WS42− anions leading to a distorted PdS4 square plane moiety, the W… Pd…W core being nearly linear (173.72(6)°). Synthesis of new ruthenium complexes [WS4Ru(bpy)2] and [WS4(Ru(bpy)2)2][PF6]2 are also reported." @default.
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- W2076103246 date "1990-02-01" @default.
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- W2076103246 title "Derivatives of tetrathiometallates. Synthesis of [MS4M′(bpy)2] (M = Mo, W; M′ = Co, Ni, Mn, Ru) complexes. Structural characterization of [Ni(bpy)3] [(WS4)2Pd]" @default.
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- W2076103246 doi "https://doi.org/10.1016/s0020-1693(00)80939-1" @default.
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