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- W2076109631 abstract "Abstract Preservative concentration in pentachlorophenol (PCP) treated wood has been traditionally determined in the industry using x-ray spectrometry or titrametric analysis of chloride. Although the methods are simple and inexpensive, they have a number of drawbacks. One of the main limitations is that the individual concentration of PCP, tetrachlorophenol (TCP), and other chlorinated chemicals cannot be determined. They are also sensitive to interferences. In the present study, procedures were developed to analyze PCP, TCP, pentachloroanisole (PCA) and trichlorophenols using gas chromatography-mass spectrometry (GC-MS). The wood to be analyzed was ground into sawdust and extracted with methanol/acetic acid in a sonicator. The extract was then pre-purified using either a FlorisilTM column (for softwood samples) or an ion exchange column (for heartwood samples) before GC-MS analysis. No PCA or trichlorophenols were detected in eight jackpine poles which has been in service for 13-37 years. The concentrat..." @default.
- W2076109631 created "2016-06-24" @default.
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- W2076109631 date "1994-10-01" @default.
- W2076109631 modified "2023-09-23" @default.
- W2076109631 title "A New Procedure for the Analysis of Chlorophenols in Preservative Treated Utility Poles" @default.
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- W2076109631 doi "https://doi.org/10.1080/03067319408033103" @default.
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