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• W2076176507 abstract "Abstract Reactions of mixed ligands succinic acid (H 2 suc) and bent dipyridines, such as 2,5‐bis(3‐pyridyl)‐1,3,4‐oxadiazole (3‐bpo) and its 4‐ N ‐donor analog (4‐bpo), with inorganic Cu II , Ni II , and Cd II salts yield three new metal‐organic coordination frameworks {[Cu(suc)(3‐bpo)(H 2 O) 2 ] · (H 2 O) 1.75 } n ( 1 ), {[Ni(suc)(4‐bpo)(H 2 O) 2 ] · (H 2 O) 5 } n ( 3 ), and {[Cd 2 (suc) 2 (3‐bpo) 2 (H 2 O) 2 ] · (H 2 O) 6.75 } n ( 4 ), in which the metal centers are linked by bridging ligands 3‐bpo/4‐bpo and suc 2– along two directions to form 2D infinite networks. The corrugated 2D nets of 1 and 4 , obtained under hydrothermal conditions, align in an interdigitated manner with the presence of significant aromatic‐stacking interactions to result in similar 3D architectures. The 2D sheets in 3 are extended by interlayer hydrogen bonds to afford a 3D structure. However, when succinic acid is replaced by fumaric acid (H 2 fum) in the reaction with 3‐bpo and Cu II salt, a metallacyclophane [Cu(Hfum) 2 (3‐bpo)(H 2 O)] 2 · (3‐bpo) 2 · (H 2 O) 6 ( 2 ) is generated. The binuclear coordinated motifs are hydrogen‐bonded to the lattice water chains to furnish a unique 3D channel‐like framework, in which the guest 3‐bpo molecules are accommodated. The thermal stabilities of these new materials were investigated by thermogravimetric analysis (TGA) of mass loss. The magnetic coupling in complexes 1 – 3 is antiferromagnetic and very small, which is as expected considering the long organic bridges between the paramagnetic centers. The solid‐state luminescence properties of 4 reveal an intense fluorescence emission at 378 nm. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2006)" @default.
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• W2076176507 date "2006-03-01" @default.
• W2076176507 modified "2023-09-23" @default.
• W2076176507 title "Novel Metallosupramolecular Networks Constructed from Cu^II, Ni^II, and Cd^II with Mixed Ligands: Crystal Structures, Fluorescence, and Magnetism" @default.
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• W2076176507 doi "https://doi.org/10.1002/ejic.200500822" @default.
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