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• W2076191567 endingPage "344" @default.
• W2076191567 startingPage "335" @default.
• W2076191567 abstract "Various digestion or extraction processes are available for the determination of trace metals in environmental samples using diverse analytical techniques. Our research examines the most efficient and reproducible methods of digestion utilising readily available laboratory equipment, reagents and instrumentation. Extraction procedures reported in over 80 recent research works were considered and the most common methods were critically evaluated. Thus nitric acid, nitric acid/perchloric acid, aqua regia, nitric acid/hydrogen peroxide and microwave-assisted methods were investigated using soil and leaf samples collected adjacent to three old metalliferous workings. Analysis was carried out using Flame Atomic Absorption Spectrometry and the results were evaluated. Differences in efficiency of extraction relative to specific metals and different substrates are highlighted and recommendations made for a digestion procedure suitable for environmental samples. Aqua regia produced the most accurate, efficient and reproducible results; we consider methods of improving both of these factors and sample preparation. Our recommended methodology has applications in environmental surveys, environmental geology, environmental toxicology, geochemistry and provides a means of obtaining meaningful and reliable results for the determination of metals present in soils, minerals and vegetation." @default.
• W2076191567 created "2016-06-24" @default.
• W2076191567 creator A5045785695 @default.
• W2076191567 creator A5068889798 @default.
• W2076191567 creator A5084609344 @default.
• W2076191567 date "2005-07-01" @default.
• W2076191567 modified "2023-10-16" @default.
• W2076191567 title "An evaluation of procedures for the digestion of soils and vegetation from areas with metalliferous pollution" @default.
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• W2076191567 doi "https://doi.org/10.1080/02772240500165570" @default.
• W2076191567 hasPublicationYear "2005" @default.
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