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• W2076192432 endingPage "974" @default.
• W2076192432 startingPage "969" @default.
• W2076192432 abstract "In this work, the (Ba1−xCax)(Ti0.94Sn0.03Zr0.03)O3 (BCTSZ-x) lead-free ceramics were prepared by the conventional solid-state method, and effects of Ca2+ content on their phase structure, microstructure, and electrical properties were investigated. The phase structure of the ceramics endures a series of the phase transitions from orthorhombic, orthorhombic–tetragonal, to tetragonal phase as the Ca2+ content increases. Their grain size gradually drops as the Ca2+ continues increasing, the dense microstructure is developed, and the Ba2+, Ca2+, Ti4+, Sn4+, and Zr4+ are homogenously distributed in the ceramic matrix. In addition, adding Ca2+ can not decrease the Curie temperature of the BCTSZ-x ceramics. Enhanced dielectric, ferroelectric, and piezoelectric properties (e.g., εr ∼ 3783, tan δ ∼ 1.3%, Pr ∼ 11.1 μC/cm2, d33 ∼ 359, and kp ∼ 0.45) were observed in the ceramic with x = 0.08 owing to the involved O–T phase boundary. As a result, the addition of Ca2+ can effectively enhance the piezoelectricity of barium titanate-based ceramics without the decrease of TC." @default.
• W2076192432 created "2016-06-24" @default.
• W2076192432 creator A5003086993 @default.
• W2076192432 creator A5055613722 @default.
• W2076192432 date "2014-12-01" @default.
• W2076192432 modified "2023-10-16" @default.
• W2076192432 title "Phase transition, microstructure, and electrical properties of Ca, Zr, and Sn-modified BaTiO 3 lead-free ceramics" @default.
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• W2076192432 doi "https://doi.org/10.1016/j.jallcom.2014.06.177" @default.
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