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• W2076233129 startingPage "1094" @default.
• W2076233129 abstract "The effect of temperature on the complex shear modulus (G*(ω)) of a model reversible covalent network formed by the Diels–Alder reaction was studied. The gel temperature of 119°C and the functional group conversion at this temperature were determined by the Winter–Chambon criterion. The complex modulus of the cross-linked network was measured from 110°C to 121°C, near the gel temperature, to determine the frequency ranges over which stress relaxation could occur. The crossover time was found to have a strong dependence on temperature (Ea ∼ 260 kJ mol–1); greater than would be expected from a typical thermally-activated retro-Diels–Alder process. Low frequency scaling of G*(ω) over the experimental frequency and temperature range was interpreted to be a result of the existence of a distribution of transient clusters in these thermoreversible covalent gels." @default.
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• W2076233129 date "2011-01-01" @default.
• W2076233129 modified "2023-09-23" @default.
• W2076233129 title "Temperature Dependent Stress Relaxation in a Model Diels–Alder Network" @default.
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• W2076233129 doi "https://doi.org/10.1071/ch11176" @default.
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