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- W2076252014 abstract "Crystalline form I (monoclinic) and form II (triclinic) of ferrocene dicarboxylic acid [Fe(η5-C5H4COOH)2] have been employed in solid−gas reactions at room temperature with the gaseous bases NH3, NH2(CH3), and NH(CH3)2. The two crystal forms behave in exactly the same way in the solid−gas reaction, generating the same products, identified as the anhydrous crystalline salts [NH4]2[Fe(η5-C5H4COO)2] (1), [NH3CH3]2[Fe(η5-C5H4COO)2] (2), and [NH2(CH3)2]2[Fe(η5-C5H4COO)2] (3). Interestingly though, all these crystals revert via vapor release exclusively to the metastable crystalline form I. Starting materials and products have been investigated by single-crystal and powder diffraction and by 13C, 15N CPMAS and 1H MAS methods." @default.
- W2076252014 created "2016-06-24" @default.
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- W2076252014 date "2006-08-18" @default.
- W2076252014 modified "2023-09-24" @default.
- W2076252014 title "A Solid−Gas Route to Polymorph Conversion in Crystalline [Fe<sup>II</sup>(η<sup>5</sup>-C<sub>5</sub>H<sub>4</sub>COOH)<sub>2</sub>]. A Diffraction and Solid-State NMR Study" @default.
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- W2076252014 doi "https://doi.org/10.1021/om060468w" @default.
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