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- W2076253804 abstract "Abstract In an attempt to obtain chiral single crystals of a two-dimensional (2D) bimetallic oxalate-based material by enantioselective auto-assembling of Mn2+ and (rac)-[Cr(C2O4)3]3− templated by the optically active complex (+)-(Rp)-[1-CH2(n-C3H7)3-2-CH3(C5H3)Fe(C5H5)]+, we obtained the unexpected 2D network species {NH(n-C3H7)3[MnCr(C2O4)3]}. X-ray diffraction determination of the structure reveals that the complex crystallizes in the enantiomorphous space group P63. The interlayer spacing of 7.93 Å is the lowest found so far for 2D, bimetallic, oxalate-bridged compounds. Keywords: ChiralityOxalate2D networksEnantioselectivitySelf-assemblingCrystal structure Acknowledgments We thank the University Pierre et Marie Curie, CNRS and the Russian Academy of Sciences (Program of Akademician R. Z. Sagdeev) for financial support. This work was supported by the CNRS/Russian Academy of Sciences agreement No. 9331 and by the RFBR grant No. 02-03-33283. Supplementary material A CIF file for the crystal structure of {NH(n-C3H7)3[MnCr(C2O4)3]} has been deposited with the Cambridge Crystallographic Data Centre, CCDC No. 227403." @default.
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- W2076253804 date "2004-09-10" @default.
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- W2076253804 title "Unexpected formation of chiral single crystals of {NH(<i>n-</i>C<sub>3</sub>H<sub>7</sub>)<sub>3</sub>[Mn<sup>II</sup>Cr<sup>III</sup>(C<sub>2</sub>O<sub>4</sub>)<sub>3</sub>]}, A 2D oxalate-based material" @default.
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