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• W2076261310 abstract "A novel diffusion-edited 3D NMR experiment that incorporates a BEST-HMQC pulse sequence in its implementation is presented. Heteronuclear 3D DOSY NMR experiments are useful in elucidating the diffusion coefficients of individual constituents of a mixture, especially in cases where the proton NMR 2D DOSY spectra show considerable overlap. The present 3D BEST-DOSY pulse sequence provides a more sensitive and less time-consuming alternative to standard 3D HMQC-DOSY experiments. Cleanly separated subspectra of individual mixture components are obtained, leading to the determination of diffusion coefficients with better accuracy. The feasibility of the technique is demonstrated on a mixture of amino acids, on a mixture of small molecules with similar diffusion coefficients, and on a complex mixture with large dynamic range (commercial gasoline). The implications of using adiabatic decoupling schemes and band-selective shaped pulses for selective BEST-DOSY experiments on proteins are also discussed." @default.
• W2076261310 created "2016-06-24" @default.
• W2076261310 creator A5001170411 @default.
• W2076261310 creator A5063709778 @default.
• W2076261310 date "2011-12-01" @default.
• W2076261310 modified "2023-10-16" @default.
• W2076261310 title "Resolving overlaps in diffusion encoded spectra using band-selective pulses in a 3D BEST-DOSY experiment" @default.
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• W2076261310 doi "https://doi.org/10.1016/j.jmr.2011.08.038" @default.
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