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- W2076278654 abstract "Dichlorocarbene, generated from base-catalysed decomposition of chloroform, adds to the double bond of 2-methylisoquinolin-1-one (1), to give the 1:1 adduct (2). The latter adduct reacts with water to give E-3-(formylmethylene)-2-methylisoindolinone (3a). Refluxing of 2 in alcohols yields alkoxybenzazepin-1-ones. Upon heating (of 2) in dimethoxyethane and subsequent reduction with lithium borohydride, 4-chloro-2-methyl-1H-2,3-dihydro-2-benzazepinone (10) was obtained as the main product. Mechanisms for the formation of these products are discussed." @default.
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- W2076278654 date "1980-01-01" @default.
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- W2076278654 title "Functionalized enamines XXIX. Solvolytic transformations of 2-methylisoquinolin-1-one dichlorocarbene adduct. Synthesis of benzazepinones" @default.
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- W2076278654 doi "https://doi.org/10.1002/recl.19800990905" @default.
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