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- W2076304867 abstract "Crystals of the double sulfate CaMg2(SO4)3 have been obtained by solid-state reactions of stoichiometric amounts of anhydrous CaSO4 and MgSO4 in sealed and evacuated silica tubes with chlorine gas as mineraliser. The crystal structure was determined from single crystal X-ray diffractometer data [P 63/m, Z = 2, a = 8.3072(4), c = 7.3057(8) A, R [F2 > 2σ (F2)] = 0.0317, wR (F2 all) = 0.0785, 476 structure factors, 33 variable parameters] and consists of distorted [CaO6] octahedra (3 symmetry), [MgO6] octahedra (3 symmetry) and SO4 tetrahedra (m symmetry) as single building units. The structure is made up of 1∞[CaO6/2] chains of face-sharing [CaO6] octahedra that extend parallel to [001], alternating with columns of face-sharing [MgO3/1O3/2]2 dimers. Both types of chains are linked via corner-sharing with SO4 tetrahedra into a three-dimensional framework structure. Although the compound crystallizes in a new structure type, it is topologically related to the NaZr2(PO4)3 (Nasicon) structure, and a comparative discussion between both structural arrangements is given. (© 2007 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)" @default.
- W2076304867 created "2016-06-24" @default.
- W2076304867 creator A5058070501 @default.
- W2076304867 date "2008-01-29" @default.
- W2076304867 modified "2023-09-26" @default.
- W2076304867 title "ChemInform Abstract: Single Crystal Growth of CaMg2(SO4)3via Solid-/Gas-Phase Reactions and Its Nasicon-Related Crystal Structure." @default.
- W2076304867 cites W2950938056 @default.
- W2076304867 doi "https://doi.org/10.1002/chin.200805005" @default.
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