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- W2076333810 abstract "Abstract Mixed-valence oxo-centered trinuclear iron carboxylate complexes with long alkyl-chain fatty acid anions, myristate [Fe 3 O(O 2 CC 13 H 27 ) 6 (py) 3 ], palmitate [Fe 3 O(O 2 CC 15 H 31 ) 6 (py) 3 ], stearate [Fe 3 O(O 2 CC 17 H 35 ) 6 (py) 3 ], and pyridine-solvated stearate [Fe 3 O(O 2 CC 17 H 35 ) 6 (py) 3 ]py, were studied by means of 57 Fe Mossbauer spectroscopy. Each nonsolvated complex showed a temperature-dependent valence transformation between being valence-detrapped at room temperature (r.t.) and valence-trapped at low temperatures, while the solvated stearate complex showed a trapped-valence state at any temperature below r.t. The complexes showed no thermal anomaly in their DSC thermograms in the temperature range of 100–298 K, although the temperature dependence of the Mossbauer parameters and the powder X-ray diffraction patterns suggested a phase transition in the solvated stearate complex at ∼190 K." @default.
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- W2076333810 date "1999-08-01" @default.
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- W2076333810 title "Mixed-valence states of iron long-chain carboxylate complexes" @default.
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- W2076333810 doi "https://doi.org/10.1016/s0020-1693(99)00124-3" @default.
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