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• W2076368654 abstract "NMR spectra of molecules oriented in liquid crystals provide homo- and heteronuclear dipolar couplings and thereby the geometry of the molecules. Several inequivalent dilute spins such as 13C and 15N coupled to protons form different coupled spin systems in their natural abundance and appear as satellites in the proton spectra. Identification of transitions belonging to each spin system is essential to determine heteronuclear dipolar couplings, which is a formidable task. In the present study, using 15N-1H and 13C-1H HSQC, and HMQC experiments we have selectively detected spectra of each rare spin coupled to protons. The 15N-1H and 13C-1H dipolar couplings have been determined in the natural abundance of 13C and 15N for the molecules pyrazine, pyrimidine and pyridazine oriented in a thermotropic liquid crystal." @default.
• W2076368654 created "2016-06-24" @default.
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• W2076368654 date "2006-01-01" @default.
• W2076368654 modified "2023-09-23" @default.
• W2076368654 title "Determination of natural abundance15N–1H and13C–1H dipolar couplings of molecules in a strongly orienting media using two-dimensional inverse experiments" @default.
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• W2076368654 doi "https://doi.org/10.1002/mrc.1791" @default.
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• W2076368654 hasPublicationYear "2006" @default.
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