Matches in SemOpenAlex for { <https://semopenalex.org/work/W2076398330> ?p ?o ?g. }
- W2076398330 endingPage "56" @default.
- W2076398330 startingPage "50" @default.
- W2076398330 abstract "Analysis of glucose and other carbohydrates are often performed by use of normal phase HPLC methods with acetonitrile as major eluent coupled with evaporative light-scattering detector (ELSD) or by use of anion-exchange ion chromatography (IC) methods with NaOH as eluent coupled with pulsed amperimetric electrochemical detector. In this work, a novel method for the determination of carbohydrates by IC in conjunction with a self-regenerating suppressor and an ELSD detector was investigated. Three carbohydrates (glucose, fructose, and sucrose) were separated using a KOH eluent generator to avoid the effect of carbon dioxide absorption in the alkaline eluent. Due to the use of the suppressor, non-volatile components were removed and a low salt background (K+ ∼0.070 μg/mL) can be obtained so the suppressed eluent could directly go into an ELSD detector without obvious interference of inorganic salts. After examining the changes in retention and resolution, an optimized method was established (for IC: using 32 mM KOH as the eluent at a flow rate of 1 mL/min; for ELSD: operated at 95 °C, 4.0 bar nitrogen with a gas flow rate of 2.0 L/min) and the linearity, reproducibility, and the limit of detection (LOD) for the three carbohydrates were further evaluated. Regression equations revealed acceptable linearity (correlation coefficients = 0.994–0.998) across the working-standard range (100–1000 μg/mL for glucose and sucrose, 150–1000 μg/mL for fructose) and LODs of glucose, fructose, and sucrose were 93, 126, and 90 μg/mL, respectively. This method has successfully been applied to the determination of the three carbohydrates in carbonated cola drinks and fruit juices. The recoveries were between 95 and 113% (n = 3) for different carbohydrates." @default.
- W2076398330 created "2016-06-24" @default.
- W2076398330 creator A5037201495 @default.
- W2076398330 creator A5056496709 @default.
- W2076398330 creator A5070695035 @default.
- W2076398330 date "2007-06-01" @default.
- W2076398330 modified "2023-10-17" @default.
- W2076398330 title "Separation and determination of carbohydrates in drinks by ion chromatography with a self-regenerating suppressor and an evaporative light-scattering detector" @default.
- W2076398330 cites W1567169386 @default.
- W2076398330 cites W1970528770 @default.
- W2076398330 cites W1975125810 @default.
- W2076398330 cites W1976035852 @default.
- W2076398330 cites W1977884934 @default.
- W2076398330 cites W1980457052 @default.
- W2076398330 cites W1988420174 @default.
- W2076398330 cites W1989721895 @default.
- W2076398330 cites W1990294315 @default.
- W2076398330 cites W1991208473 @default.
- W2076398330 cites W1991889956 @default.
- W2076398330 cites W2000741452 @default.
- W2076398330 cites W2008981922 @default.
- W2076398330 cites W2011799661 @default.
- W2076398330 cites W2017038281 @default.
- W2076398330 cites W2018002735 @default.
- W2076398330 cites W2036232758 @default.
- W2076398330 cites W2039613283 @default.
- W2076398330 cites W2044173253 @default.
- W2076398330 cites W2045388602 @default.
- W2076398330 cites W2045471156 @default.
- W2076398330 cites W2052154575 @default.
- W2076398330 cites W2052616752 @default.
- W2076398330 cites W2057319211 @default.
- W2076398330 cites W2057404913 @default.
- W2076398330 cites W2057432190 @default.
- W2076398330 cites W2071044431 @default.
- W2076398330 cites W2080992711 @default.
- W2076398330 cites W2081135573 @default.
- W2076398330 cites W2082129916 @default.
- W2076398330 cites W2082214675 @default.
- W2076398330 cites W2083173300 @default.
- W2076398330 cites W2090459887 @default.
- W2076398330 cites W2138775239 @default.
- W2076398330 cites W2142631151 @default.
- W2076398330 doi "https://doi.org/10.1016/j.chroma.2007.02.080" @default.
- W2076398330 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/17374373" @default.
- W2076398330 hasPublicationYear "2007" @default.
- W2076398330 type Work @default.
- W2076398330 sameAs 2076398330 @default.
- W2076398330 citedByCount "31" @default.
- W2076398330 countsByYear W20763983302012 @default.
- W2076398330 countsByYear W20763983302013 @default.
- W2076398330 countsByYear W20763983302015 @default.
- W2076398330 countsByYear W20763983302016 @default.
- W2076398330 countsByYear W20763983302017 @default.
- W2076398330 countsByYear W20763983302021 @default.
- W2076398330 countsByYear W20763983302022 @default.
- W2076398330 crossrefType "journal-article" @default.
- W2076398330 hasAuthorship W2076398330A5037201495 @default.
- W2076398330 hasAuthorship W2076398330A5056496709 @default.
- W2076398330 hasAuthorship W2076398330A5070695035 @default.
- W2076398330 hasConcept C110084920 @default.
- W2076398330 hasConcept C113196181 @default.
- W2076398330 hasConcept C118859902 @default.
- W2076398330 hasConcept C119128265 @default.
- W2076398330 hasConcept C179998833 @default.
- W2076398330 hasConcept C185592680 @default.
- W2076398330 hasConcept C206967267 @default.
- W2076398330 hasConcept C2776970464 @default.
- W2076398330 hasConcept C2778597767 @default.
- W2076398330 hasConcept C43617362 @default.
- W2076398330 hasConcept C51724486 @default.
- W2076398330 hasConcept C55493867 @default.
- W2076398330 hasConceptScore W2076398330C110084920 @default.
- W2076398330 hasConceptScore W2076398330C113196181 @default.
- W2076398330 hasConceptScore W2076398330C118859902 @default.
- W2076398330 hasConceptScore W2076398330C119128265 @default.
- W2076398330 hasConceptScore W2076398330C179998833 @default.
- W2076398330 hasConceptScore W2076398330C185592680 @default.
- W2076398330 hasConceptScore W2076398330C206967267 @default.
- W2076398330 hasConceptScore W2076398330C2776970464 @default.
- W2076398330 hasConceptScore W2076398330C2778597767 @default.
- W2076398330 hasConceptScore W2076398330C43617362 @default.
- W2076398330 hasConceptScore W2076398330C51724486 @default.
- W2076398330 hasConceptScore W2076398330C55493867 @default.
- W2076398330 hasIssue "1" @default.
- W2076398330 hasLocation W20763983301 @default.
- W2076398330 hasLocation W20763983302 @default.
- W2076398330 hasOpenAccess W2076398330 @default.
- W2076398330 hasPrimaryLocation W20763983301 @default.
- W2076398330 hasRelatedWork W2012687781 @default.
- W2076398330 hasRelatedWork W2061196676 @default.
- W2076398330 hasRelatedWork W2113356700 @default.
- W2076398330 hasRelatedWork W2160690438 @default.
- W2076398330 hasRelatedWork W2274111671 @default.
- W2076398330 hasRelatedWork W2370021892 @default.
- W2076398330 hasRelatedWork W2375283334 @default.
- W2076398330 hasRelatedWork W2377649415 @default.
- W2076398330 hasRelatedWork W2388095329 @default.