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• W2076455212 abstract "Abstract The reaction of the bifunctional ligand 3-(1,8-naphthalimido)propanoate ( L C2 − ), which combines a 1,8-naphthalimide strong π ··· π stacking synthon and a carboxylate donor group, with Zn( O 2 CCH 3 ) 2 (H 2 O) 2 in methanol yields trimetallic Zn 3 ( L C2 ) 6 (MeOH) 4 . The solid state structure has a central zinc(II) linked to two equivalent outer zinc(II) by both μ-κ 1 and μ-κ 2 carboxylate ligands. The two equivalent five-coordinate terminal zinc centers are also bonded to a third nonbridging κ 2 -carboxylate and to the oxygen atom of a methanol molecule. The central zinc(II) is six-coordinate with the four bridging carboxylate oxygen atoms forming a square planar arrangement and two trans oriented methanol molecules completing the coordination sphere. These trimers are organized into an extended structure exclusively by noncovalent interactions. Two types of strong π ··· π stacking interactions between sets of three stacked naphthalimide rings from three different trinuclear molecules organize the structure into two-dimensional thick sheets. The third dimension is organized by intermolecular hydrogen bonding interactions between the methanol molecules bonded to the terminal zinc(II) and the free oxygen of the μ-κ 1 -carboxylates from adjacent trimeric units. This interaction is supported by weak π ··· π stacking. Overall the structure is a highly organized supramolecular metal–organic framework (SMOF) solid." @default.
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• W2076455212 date "2010-12-01" @default.
• W2076455212 modified "2023-09-24" @default.
• W2076455212 title "Synthesis and structure of a zinc(II)-carboxylate trimer containing the π···π stacking, 1,8-naphthalimide synthon: A supramolecular metal–organic framework" @default.
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• W2076455212 doi "https://doi.org/10.1016/j.ica.2010.05.039" @default.
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