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- W2076561404 abstract "A method for analysis of mixtures of 3-hexuloses by gas chromatography mass spectrometry of their di-O-isopropylidene derivatives has been elaborated. The origin of characteristic fragment ions in the mass spectra is suggested on the basis of the spectra of d(12) analogues, obtained by acetonation with acetone-d(6) and on MS/MS investigations. The method has been applied to product mixtures from aldol reactions between glycero-tetrulose and glycolaldehyde and between 2-pentuloses and formaldehyde. An interesting result is the formation of ribo-3-hexulose with a high degree of stereoselectivity in alkali catalysed reaction between erythro-2-pentulose and formaldehyde." @default.
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- W2076561404 date "2004-09-01" @default.
- W2076561404 modified "2023-10-17" @default.
- W2076561404 title "Formation of 3-hexuloses in aldol reactions, analysis of the products as their O-isopropylidene derivatives by GC–MS" @default.
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- W2076561404 doi "https://doi.org/10.1016/j.carres.2004.06.018" @default.
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