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- W2076579894 abstract "Abstract The title compound was synthesized by reaction of N-(azidomethyl)thiourea or N-(tosylmethyl)thiourea with α -phenylsulfonylacetophenone in the presence of sodium hydride followed by p -toluenesulfonic acid treatment of the obtained N-[3-oxo-3-phenyl-2-(phenylsulfonyl)propyl]thiourea. The molecular and crystal structure of 6-phenyl-5-phenylsulfonyl-1,2,3,4-tetrahydropyrimidine-2-thione (C 14 H 13 N 2 S 2 O 2 ; space group P2 1 / a ; Z =4; a =17.396(1) Å, b =5.887(1) Å, c =15.665(2) Å, β =104.89(1) o ) have been determined and refined from neutron (the neutron diffraction was very effective for describing of this system due to using of partial hydrogen-deuterium substitution) powder diffraction data using grid search and a Rietveld procedures. The crystal structure is formed by centrosymmetric hydrogen-bonded dimers along a axis." @default.
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- W2076579894 date "2001-12-01" @default.
- W2076579894 modified "2023-09-27" @default.
- W2076579894 title "Synthesis and crystal structure determination of 6-phenyl-5-phenylsulfonyl-1,2,3,4-tetrahydropyrimidine-2-thione from neutron powder diffraction data" @default.
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- W2076579894 doi "https://doi.org/10.1524/zkri.216.12.629.22491" @default.
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