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- W2076597849 abstract "Flash vacuum pyrolysis of bis(trimethylsilylmethyl)methoxysilanes was found to be an efficient route to 1,3-disilacyclobutanes. Flash vacuum pyrolysis of bis(trimethylsilylmethyl)dimethoxysilane or bis(trimethylsilylmethyl)chloromethoxysilane gave 1-methoxy-1,3,3-trimethyl-1,3-disilacyclobutane or 1-chloro-1,3,3-trimethyl-1,3-disilacyclobutane, respectively. The thermolysis is regarded as proceeding through initial β-elimination of trimethylmethoxysilane followed by intramolecular cyclization of the resulting 2-methoxy-4,4-dimethyl-2,4-disilapent-1-ene or 2-chloro-4,4-dimethyl-2,4-disilapent-1-ene to give the products." @default.
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- W2076597849 date "1992-10-01" @default.
- W2076597849 modified "2023-09-27" @default.
- W2076597849 title "A convenient synthesis of 1,3-disilacyclobutanes" @default.
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- W2076597849 doi "https://doi.org/10.1016/0022-328x(92)85073-6" @default.
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