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- W2076625765 abstract "The X-ray crystal structure of the first bridged complex of rhodium with coordinated nbd [(μ-OSiMe3)Rh(nbd)]2 (I) was determined at room temperature. The reaction of I with triphenylphosphine gave monomeric and dimeric products whose formula depends on the [Rh]:[P] ratio, i.e. [Rh(μ-OSiMe3)(nbd)PPh3] (III), for [Rh]:[P] = 1:1 and [(μ-OSiMe3)Rh(PPh3)2] (IV) where [Rh]:[P] = 1:2. The reaction of I with an excess of triethylsilane yielded [RhH2SiEt3(nbd)] (VI) with elimination of triethyltrimethyldisiloxane. The reaction of III with triethylsilane furnished finally VI. Formation of all complexes was followed by 1H and 31P NMR spectroscopy as well as by GC-MS." @default.
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- W2076625765 date "1996-09-01" @default.
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- W2076625765 title "The structure and some reactions of di-μ-trimethylsilyloxy-bis-(norborna-2,5-diene)-dirhodium(I)" @default.
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- W2076625765 doi "https://doi.org/10.1016/0277-5387(96)00156-8" @default.
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