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- W2076642288 abstract "Reconcentration of samples by solvent evaporationis problematic if the solutes of interest are of up to intermediate volatility: substances with up to surprisingly high boiling points (exceeding 250°C) may be lost by co-evaporation. There is poor control over such losses and analytical results are of accordingly limited reliability. Solvent/solute evaporation is described as a gas chromatographic process. Retaining liquid such as (re-)condensed solvent should be ahead of the evaporation site in order to retain otherwise escaping solute material. However, before investing in tedious procedures, it is recommended that one should consider instead on-column injection of increased sample volumes as solvent evaporation carried out in the column inlet (retention gap) virtually precludes losses of solute material, combining optimal performance with simplicity (sample reconcentration in the conventional sense is circumvented)." @default.
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- W2076642288 date "1987-01-01" @default.
- W2076642288 modified "2023-10-07" @default.
- W2076642288 title "Sample reconcentration by column-external solvent evaporation or injection of large volumes into gas chromatographic capillary columns?" @default.
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- W2076642288 doi "https://doi.org/10.1016/s0021-9673(01)86867-9" @default.
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