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- W2076713498 abstract "Abstract A simple approach to generating in situ metal‐templated tris‐(2‐picolyl)amine‐like multicomponent assemblies with potential applications in molecular recognition and sensing is reported. The assembly is based on the reversible covalent association between di‐(2‐picolyl)amine and aldehydes. Zinc ion is best for inducing assembly among the metal salts investigated, whereas 2‐picolinaldehyde is the best among the heterocyclic aldehydes studied. Although an equilibrium constant of 6.6×10 3 M −1 was measured for the assembly formed by 2‐picolinaldehdye, di‐(2‐picolyl)amine, and zinc triflate, the equilibrium constants for other systems are in the 10 2 M −1 range. X‐ray structural analysis revealed that zinc adopts trigonal‐bipyramidal geometry within the assembled ligand. The diversity and equilibrium of the assemblies are readily altered by simply changing concentrations, varying components, or adding counteranions." @default.
- W2076713498 created "2016-06-24" @default.
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- W2076713498 date "2011-08-23" @default.
- W2076713498 modified "2023-10-18" @default.
- W2076713498 title "Dynamic Multicomponent Hemiaminal Assembly" @default.
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- W2076713498 doi "https://doi.org/10.1002/chem.201101085" @default.
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