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- W2076753093 abstract "Abstract Porous crystals of magnetite and vacancy-ordered maghemite, rhombohedron-shaped, reaching 150 μm in size, and having remarkably large specific surface area (88.55 m2/g for magnetite, 40.14 m2/g for maghemite) were obtained via topotactical conversion, starting from hydrothermally grown siderite single crystals. The increase in density (from 3.9 g/cm3 for siderite to 5.24 g/cm3 for magnetite and 4.9 g/cm3 for maghemite) caused quasi-ordered internal pores-grains pattern, with mesocrystalline appearance. The X-ray Line-Profile Fitting-based microstructure analysis gave 64±6 nm and 84±8 nm for the average inner grains size in magnetite and maghemite. Structure and phase content analysis indicated high purity and crystallinity. Magnetic measurements indicated saturation magnetization (92.1 emu/g for magnetite and 85.5 emu/g for maghemite) approaching the upper limits reported for the pure bulk oxides." @default.
- W2076753093 created "2016-06-24" @default.
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- W2076753093 date "2013-10-01" @default.
- W2076753093 modified "2023-10-17" @default.
- W2076753093 title "Highly crystalline porous magnetite and vacancy-ordered maghemite microcrystals of rhombohedral habit" @default.
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- W2076753093 doi "https://doi.org/10.1016/j.jcrysgro.2013.06.003" @default.
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