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- W2076806914 abstract "The preparation of tetrabutyltin by a Wurtz reaction from stannic chloride, butyl chloride and sodium is described. To avoid losses of tin, due to the reduction of stannic chloride, a cyclic process is developed: instead of stannic chloride, dibutyltin dichloride is used as a starting material in the Wurtz reaction. The tetrabutyltin obtained is treated with stannic chloride to give dibutyltin dichloride, part of which has to be recycled. The disproportionation reaction used in the preparation of dibutyltin dichloride from tetrabutyltin and the chlorination of hexabutyldistannane, obtained as a by-product in the Wurtz reaction, are briefly dealt with." @default.
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- W2076806914 date "2007-05-04" @default.
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- W2076806914 title "Investigations on organo-tin compounds. I. The preparation of butyltin compounds by a Wurtz reaction" @default.
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- W2076806914 doi "https://doi.org/10.1002/jctb.5010040605" @default.
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